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Vapor-phase osmometry has been used for molecular mass measurements of polymers using the commercial instrumentation that is used to evaluate the molecular masses of monomeric molecules (11). Drops of solution and solvent are measured with thermistors in a temperature-controlled cavity that is saturated with vapors of the solvent. A solution has a lower vapor pressure, and the heat of condensation causes the temperature of the drop to rise until the solution vapor pressure is increased and equal to that of the solvent. In actuality, this does not happen as a state of equilibrium is reached when the heat losses from the drops become equal to the heat of condensation of the solvent. The increase in temperature is directly proportional to the molality of the solute. A schematic of a vapor-phase osmometer is shown in Figure 3.18. The temperature is controlled to about 1/1000 C. The difference in temperature is measured with a circuit that measures resistance changes ( R) quite precisely. Starting with a species of known molecular mass, a calibration curve of the molality (m) vs. R is constructed and then the unknown molecular mass is determined from the R

3:7-14

Long Exit:

The reason for this is that regular insulin takes 15 to 30 minutes before it starts to work Because rapid-acting insulin acts, as the name suggests, rapidly, it can be given anywhere from immediately before eating to 15 minutes before eating This makes taking rapid-acting insulin more convenient to use than regular insulin for most people Because rapid-acting insulin works so quickly, in some special circumstances it can be given after a meal Here are two situations where this is sometimes done: The young child whose eating is unpredictable As most parents of a young child know, there is no guarantee the child is going to eat all the food they are given Therefore it can be difficult to know how much mealtime insulin (the amount of which is based on the amount of carbohydrate being eaten) to give.

Interrante and coworkers (67 72) have perfected the ROP of cyclic SiCSiC ring compounds (73) and substitution reactions as shown in Figure 2.39. The dichlorosilane groups are reduced with lithium aluminum hydride to an alternating silylene-methylene chain. Poly(silylene-methylene) [SiH2 CH2 ]n has a melting temperature of about 25 C and a glass transition temperature of about 135 C, is air stable, and dissolves readily in common organic solvents. With a chloromethylsilylene group a variety of other species can be formed (Fig. 2.39). The [Si(CH3 )(OR)CH2 ]n derivatives vary in both glass transition temperatures and hydrolytic sensitivity depending on the R group (that includes ethyl, 1,1,1-tri uoroethyl, acetyl, and phenyl). Polycarbodi uorosilane [SiF2 CH2 ]n and [Si(CH3 )(CN)CH2 ]n have also been synthesized by appropriate substitution reactions (74, 75). A number of other laboratories have also reported ring-opening carbosilane polymerization reactions as detailed in a recent review (64). Even with the H2 PtCl6 catalyst, temperatures of 80 100 C or extended re ux is required for solvents that boil below that temperature range. Thus the photocatalyzed ROP of a disilacyclobutate with platinum(II) acetylacetonate at room temperature (76) (Fig. 2.40) is encouraging. Compelling evidence for both homogeneous and heterogeneous paths has been presented, although the mechanistic details are somewhat uncertain (76).

(x0,z0)

In this situation, rapid-acting insulin is sometimes (that is; not routinely) administered after the child eats; this way the parent can give the dose based on what the child actually ate, not on what it was anticipated he would eat Diabetic Gastroparesis Gastroparesis is a condition in which the stomach is damaged from longstanding diabetes and as a result doesn t properly empty its contents into the small intestine This delayed delivery of nutrients into the small intestine (from where nutrients are then absorbed into the body) results in a delayed and often unpredictable rise in blood glucose This makes it very difficult to properly estimate how much insulin to give before a meal.